In-line measuring, monitoring, and analysis is found in all process industries. Whether involving liquids or gases, in-line methodologies provide a variety of benefits over sporadic grab samples, including greater data reliability, accuracy, and consistency (primarily because of automatic calibration and verification); more, faster, repeatable measurements; fewer man-hours required; and tighter...
In-line measuring, monitoring, and analysis is found in all process industries. Whether involving liquids or gases, in-line methodologies provide a variety of benefits over sporadic grab samples, including greater data reliability, accuracy, and consistency (primarily because of automatic calibration and verification); more, faster, repeatable measurements; fewer man-hours required; and tighter control of the process. Extending these benefits are current networking and reporting functions, which add greater consistency and precision through electronic record keeping and performance validation.
"You want sensor technology in-line as much as possible," says Daryl Belock, commercial programs manager for GE Sensing. "The method offers the best representative sample. The installation is usually simple. Unlike grab samples, there is no extraneous hardware pulling a sample out of the line. And you get fast response having the sensor directly in the flow path."
The primary issues revolve around whether the sensing device is sufficiently rugged and insensitive enough to all that's going on in the process stream with respect to temperature, pressure, flow, contaminants, and corrosion.
So what makes in-line monitoring and measuring technology so popular and prevalent? In-line devices are used to measure a multitude of parameters (pressure, temperature, flow), though pH, conductivity, and dissolved oxygen are probably among the more common. The methodology is used primarily for control, points out Mel Thweatt, applications manager, analytical instrumentation at ABB Instrumentation. "In the wastewater industry, for example, you need to monitor the addition of disinfectant into the water to know how much disinfectant to add. Real-time data are needed to determine how much chemical is required to control the process. Grab samples analyzed by a lab will not suffice. There are too many variables. The composition changes too fast."
Adds Tom Griffiths, product manager for Honeywell, "People want to get away from time-consuming grab samples. The trend today is 'give me more information, faster, in a form that will make my job easier so that I can react faster and smarter.' The user is looking for more, better information to make a smarter and faster decision about the process."
In-line analysis provides just that. But other factors influence its use. In the opinion of ABB's Thweatt, one reason for in-line analysis is downsizing. "Analysis that used to be done by people in labs isn't done that way anymore," he observes. "Automated methods are taking precedence."
Honeywell's Griffiths agrees. "Fewer people in the plant make reliable and accurate in-line analysis and monitoring more important. In-line devices allow a reduction in the number of measurements and analyses that need to be done in the lab. But," he warns, "some samples must be done in the lab. The lab isn't going away. Some measurements require laboratory verification."
Stanzi Prell, marketing director, industrial, at Hach Co. sees the situation similarly. "When we compare in-line and portable laboratory instrumentation at our company, growth rate on the in-line side is definitely higher. We attribute this to personnel cutbacks. There are fewer people to conduct these tests, but tests still need to be conducted. In addition, plants want and need faster response times. They don't want to take three grab samples a day. They want to know pH values constantly in real time. This information is a great indicator about the process. It can help avoid shutting down a line or making a poor quality product."
The process of performing in-line analyses has progressed steadily, albeit slowly, continuing to respond to user demands. Sensor designs "have made incremental advancements in terms of reliability and dependability," notes Andy Szeto, product manager, analytical instrumentation, ABB Instrumentation. "However, they are based on the same principles developed in the past. It's the surrounding peripherals such as analyzers and transmitters that have changed the most. Users are looking for analyzers with more features, such as easier-to-use interfaces, diagnostics, and digital communications. Although many facilities still operate with analog transmitters, there is increasing interest in fieldbus-enabled devices, such as FOUNDATION fieldbus and Profibus. These communication protocols allow access to data that traditionally were not available with the older analog instrumentation."
GE Sensing's Belock cites wireless applications as an area that will increase, but issues remain. He notes, "Can the distance be accommodated? Will storms interfere? Is the application sensitive to electromagnetic or radio frequency interference (EMI/RFI)? Is the sensor susceptible to radio transmissions and vice versa? A lot of industrial installations aren't 'wireless-friendly.' Networking is good for reporting data but not necessarily for controlling the process, yet."
Many once-troublesome problems, however, have been overcome. Fragile glass electrodes prone to breakage can be replaced with non-glass varieties, such as Honeywell's Durafet line. The non-breakable, solid-state in-line device performs pH measurement in real time. Problems with leaks, as well, are now almost a thing of the past. Cutting into a line admittedly creates another potential leak path or point of contamination, but technology today has made leak problems minimal.
Other analyses issues, contamination for one, have been alleviated through ex-situ approaches and sample-handling systems. In-line (or in-situ ) analyses can lead to problems if a device fails. There must be a way to pull the device out of service without shutting down the process. In applications where shutdown is difficult or impossible, such as moisture analysis in a refinery, a sample panel may make more sense.
In these arrangements, explains GE Sensing's Belock, a small amount of flow is tapped off. "It's run through a sample panel—often a very simple configuration of isolation valve, filter, probe, pressure gauge, and flowmeter. The system protects the sensor and makes it more serviceable and accessible for calibration."
In ex-situ designs, the sensor resides outside the probe. Belock illustrates with a flue gas analyzer example: "We move a small amount of flow coming out of the flue gas past the sensor using a thermal convection flow loop. Because we can control the flow to a very low level, we can reduce the particulate level at the sensor, reduce plugging, and not have as many problems with sensor contamination. If the sensor does need replacement, it's not complicated because the sensor is not in the probe or probe sleeve. These systems are somewhat more expensive and the response time can be slower because you're not in-situ , but the other performance benefits outweigh the desire for an in-situ solution and the results are just as accurate."
Sometimes a sample has to be run through a cooler, or filtered to lower the temperature, before measuring, adds ABB's Szeto. It's still a continuous, online/inline measurement, but putting the sample through treatment or conditioning does add time and slow down the reading. The preferred method is still to measure directly in-line in the process to get the quickest, fastest, most reliable measurement with the least delay."
From a distance
There are lots of in-line devices and systems in use today, and that's not likely to change significantly any time soon, most agree. But, as with every technology, change will come.
Refinements for in-line devices are helping to keep them competitive even as new technologies enter the market. End-users are asking for sensors that are smarter about when they need to be cleaned, calibrated, or changed. They want diagnostic capabilities that will bring information to the operator directly from the instrument. And those demands are being met.
However, non-intrusive methods are advancing; some—ultrasonic flowmeters and optical-based instrumentation, for example—are already in use. Several vendors offer clamp-on gas analysis using ultrasonic flowmeters, but it is still relatively expensive. Hach Co.'s LDO, luminescent dissolved-oxygen probe uses optical-based technology (see photo); it has no membranes and requires virtually no end-user maintenance.
End-users today need reliable instruments that generate data they can trust to accurately reflect what's going on in a process. Technology will continue to evolve. New designs and better performance will become available, and be adopted. But the transition will be slow and steady. In-line devices will be around for a long time to come.
In-line analysis keeps power plant on cutting edge
East Kentucky Power, a coal-fired electric generating plant near Maysville, KY, is among the most progressive power plants in the region. Always on the cutting edge of technology, the company operates three units at its Spurlock Power Station location, and plans to build another in 2006. Virtually all liquid analysis is done with in-line devices; most of the facility's water sampling areas are outfitted with Honeywell devices. Products include pH, conductivity, and dissolved oxygen meters.
Presently in use are Honeywell Durafet pH probes on river water applications and older, ultra-pure pH assemblies on ultra-pure water applications inside the plant. The facility is now looking at purchasing HPW 7000 ultra-pure water equipment for the boiler water sampling areas. Recently added instrumentation includes three new pH and conductivity meters and two dissolved oxygen meters. The company also supplies steam to a nearby paper company. It uses Honeywell pH equipment on all sampling lines for that application.
Equipment is meticulously cared for by a group that has worked together for nearly 20 years. Bob Weigott, instrumentation and control manager and 30-year company veteran, guides the department and the care of equipment. The recent upgrade of devices, he explains, has been part of a gradual move to replace instruments that had become maintenance intensive. "Older analog systems tended to drift, and were a little noisy at times. They needed to be calibrated and checked far too often. We were having some problems on weekends. Some of the older instrumentation would drift and go into alarm mode and we were having to call in people to address those things on Saturdays and Sundays."
The recent upgrade has eliminated those problems, adds Matt Grooms, one of the instrumentation technicians involved in replacing the devices. "We changed out a lot of instrumentation—conductivity, dissolved oxygen, and pH devices. The new digital systems are more reliable. They stay more accurate for a longer period of time."
Our boiler chemistry must be up to par, stresses Weigott, explaining the reasons for the upgrade. "It's a very important item. Any problems are addressed immediately. The boiler is probably the most important—and expensive—equipment in a power plant. You can destroy a lot of boiler tubes if your water is too acidic. Our in-line analyzers function all the time and report back to the DCS on a continual basis. Alarms signal any problems immediately.
"Our lab people check fluid compositions every morning," he continues. "They go to the boiler sample panels and confirm that what the instrumentation is telling them is correct. If anything isn't right, we go out and calibrate those instruments. We can't jeopardize anything in that cycle. Those readings have to be extremely accurate, 24/7."
Up-to-date in-line instrumentation helps make sure they are.
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